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犌犅31604.44—2016 2016101920170419犌犅31604.44—2016 GB/T23296.18—2009《》 GB/T23296.18—2009“:——————”; Ⅰ犌犅31604.44—2016 1 2 143 GB/T66823.1 3.1.1 CHO( )2 4 2()CHO2 63.1.2 ()3.1.3 CHO4()3.1.4 CH3.1.5 7 16 :GB31604.13.2 : GB5009.1563.3 ( :)3.3.1 CHO CAS 1072113.3.2 (C4H10O3CAS :111466)3.3.3 14 (C4H10O2CAS :110634)2 6 23.4 ( /)3.4.1 7500mgL0.1mg)(/) :7500mgL0.75g(100mL0℃4℃1 1犌犅31604.44—20163.4.2 14 10000mgL(/) :1g140℃4℃(0.1mg)100mL1/)2mL 14 10000mgL3.4.3 14 800mgL(/):(25mL0℃4℃ (2mL 1410000mgL:/)3.4.4 6 25mL0.0mL0.5mL1.0mL2.5mL5.0mL10.0mL// // //0.0mgL150.0mgL300.0mgL750.0mgL1500mgL3000mgL14/800mgL0℃4℃4 ::4.1 4.2 4.3 0.0001g 0.01g 0.1g: 250mL4.4 :25mL 50mL 100mL4.5 :1mL 2mL4.6 :50mL4.7 :0.22μm 5 5.1 5.1.1 // / / / /0.0mgL3.0mgL6.0mgL15.0mgL30.0mgL60.0mgL5.1.1.1 1mL 6 50mL 5.1.1.2 50g(0.1g)6 250mL1mL/ / / / / /0.0mgkg3.0mgkg6.0mgkg15.0mgkg30.0mgkg60.0mgkg;50mL1min 5min;;20mL50mL;1mL0.2μm5.1.2 5.1.2.1 GB5009.156 GB31604.10℃4℃ 2犌犅31604.44—2016 5.1.2.2 (/)1mL 14800mgL50mL1mL5.1.2.3 50g(0.1g)250mL20mL1mL 14800mgL5min(/)1min50mL;;20mL50mL;1mL5.1.3 5.1.25.2 5.2.1 )a :30m 0.32mm1μm;b):100℃1min10℃/min 200℃8min;1mL/min;):cd):;220℃)e:0.5min;):;220℃: 1Lμfg)5.2.2 5.1.114A5.2.3 14;6 7 GB5009.15610% 3